Publicação
Avaliação da limpeza de CDtrodo construídos a partir de CD de ouro gravável/fita adesiva de galvanoplastia
| Resumo: | Gold electrodes are widely used in electrochemistry and electroanalytical chemistry, due to the high purity, broad range of work potential as well as the possibility to control and modify the surface. On this work construction and cleaning of electrodes from gold recordables compact discs (CD-Rs), namely CDtrodes, are described. The CDs was submitted to the action of concentrated HNO3 in order to remove the protection layer and to expose the metallic layer; the electrode area was delimited by using galvanoplasty tape. The literature has been published many articles on CDtrode focused on the application but not on the cleaning; there is no register on galvanoplasty tape to define electrode area. Several methods for gold surface cleaning after attack of HNO3 were investigated, such as application of fixed potential in NaCl solution, successive scans in H2SO4 and ultrasound application, and best results were obtained in H2SO4 solution. This electrode material is interesting due to the performance comparable to the commercial electrodes, besides great versatility and low cost. |
|---|---|
| Autores principais: | Foguel, M. V. |
| Outros Autores: | Uliana, C. V.; Tomaz, P. R.U.; Marques, P. R. B. Oliveira; Yamanaka, H.; Ferreira, A. A. Pupim |
| Assunto: | CDtrode, CD-R electrodes Cyclic voltammetry Gold surface cleaning |
| Ano: | 2022 |
| País: | Brasil |
| Tipo de documento: | artigo |
| Tipo de acesso: | acesso aberto |
| Instituição associada: | IBICT |
| Idioma: | português |
| Origem: | Oasisbr |
| _version_ | 1871586297135497216 |
|---|---|
| author | Foguel, M. V. |
| author2 | Uliana, C. V. Tomaz, P. R.U. Marques, P. R. B. Oliveira Yamanaka, H. Ferreira, A. A. Pupim |
| author2_role | author author author author author |
| author_facet | Foguel, M. V. Uliana, C. V. Tomaz, P. R.U. Marques, P. R. B. Oliveira Yamanaka, H. Ferreira, A. A. Pupim |
| author_role | author |
| country_str | BR |
| creators_json_txt | [{\"Person.name\":\"Foguel, M. V.\"},{\"Person.name\":\"Uliana, C. V.\"},{\"Person.name\":\"Tomaz, P. R.U.\"},{\"Person.name\":\"Marques, P. R. B. Oliveira\"},{\"Person.name\":\"Yamanaka, H.\"},{\"Person.name\":\"Ferreira, A. A. Pupim\"}] |
| datacite.creators.creator.creatorName.fl_str_mv | Foguel, M. V. Uliana, C. V. Tomaz, P. R.U. Marques, P. R. B. Oliveira Yamanaka, H. Ferreira, A. A. Pupim |
| datacite.date.Accepted.fl_str_mv | 2009-01-01T00:00:00Z |
| datacite.date.available.fl_str_mv | 2022-04-28T19:45:47Z |
| datacite.date.embargoed.fl_str_mv | 2022-04-28T19:45:47Z |
| datacite.rights.fl_str_mv | http://purl.org/coar/access_right/c_abf2 |
| datacite.subjects.subject.fl_str_mv | CDtrode, CD-R electrodes Cyclic voltammetry Gold surface cleaning |
| datacite.titles.title.fl_str_mv | Avaliação da limpeza de CDtrodo construídos a partir de CD de ouro gravável/fita adesiva de galvanoplastia |
| dc.creator.none.fl_str_mv | Foguel, M. V. Uliana, C. V. Tomaz, P. R.U. Marques, P. R. B. Oliveira Yamanaka, H. Ferreira, A. A. Pupim |
| dc.date.Accepted.fl_str_mv | 2009-01-01T00:00:00Z |
| dc.date.available.fl_str_mv | 2022-04-28T19:45:47Z |
| dc.date.embargoed.fl_str_mv | 2022-04-28T19:45:47Z |
| dc.format.none.fl_str_mv | 59-66 |
| dc.identifier.none.fl_str_mv | http://hdl.handle.net/11449/222610 |
| dc.language.none.fl_str_mv | por |
| dc.rights.none.fl_str_mv | http://purl.org/coar/access_right/c_abf2 |
| dc.source.none.fl_str_mv | reponame:Repositório Institucional da UNESP instname:Universidade Estadual Paulista (UNESP) instacron:UNESP |
| dc.subject.none.fl_str_mv | CDtrode, CD-R electrodes Cyclic voltammetry Gold surface cleaning |
| dc.title.fl_str_mv | Avaliação da limpeza de CDtrodo construídos a partir de CD de ouro gravável/fita adesiva de galvanoplastia |
| dc.type.none.fl_str_mv | http://purl.org/coar/resource_type/c_6501 |
| description | Gold electrodes are widely used in electrochemistry and electroanalytical chemistry, due to the high purity, broad range of work potential as well as the possibility to control and modify the surface. On this work construction and cleaning of electrodes from gold recordables compact discs (CD-Rs), namely CDtrodes, are described. The CDs was submitted to the action of concentrated HNO3 in order to remove the protection layer and to expose the metallic layer; the electrode area was delimited by using galvanoplasty tape. The literature has been published many articles on CDtrode focused on the application but not on the cleaning; there is no register on galvanoplasty tape to define electrode area. Several methods for gold surface cleaning after attack of HNO3 were investigated, such as application of fixed potential in NaCl solution, successive scans in H2SO4 and ultrasound application, and best results were obtained in H2SO4 solution. This electrode material is interesting due to the performance comparable to the commercial electrodes, besides great versatility and low cost. |
| dirty | 0 |
| eu_rights_str_mv | openAccess |
| format | article |
| id | oasisbr_36bd2486da360cb22ac342e60156b764 |
| identifier.url.fl_str_mv | http://hdl.handle.net/11449/222610 |
| inst_facet_str | urn:organizationAcronym:oasisbr{{{_:::_}}}IBICT |
| instacron_str | OASISBR |
| institution | IBICT |
| instname_str | IBICT |
| language | por |
| network_acronym_str | oasisbr |
| network_name_str | Oasisbr |
| oai_identifier_str | oai:repositorio.unesp.br:11449/222610 |
| organization_str_mv | urn:organizationAcronym:oasisbr |
| person_str_mv | Foguel, M. V. Uliana, C. V. Tomaz, P. R.U. Marques, P. R. B. Oliveira Yamanaka, H. Ferreira, A. A. Pupim |
| publishDate | 2022 |
| repo_facet_str | urn:repositoryAcronym:oasisbr{{{_:::_}}}Oasisbr |
| reponame_str | Oasisbr |
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| spelling | Avaliação da limpeza de CDtrodo construídos a partir de CD de ouro gravável/fita adesiva de galvanoplastiaFoguel, M. V.Uliana, C. V.Tomaz, P. R.U.Marques, P. R. B. OliveiraYamanaka, H.Ferreira, A. A. PupimCDtrode, CD-R electrodesCyclic voltammetryGold surface cleaningopen accesshttp://purl.org/coar/access_right/c_abf2http://hdl.handle.net/11449/222610HandleEcletica Quimica, v. 34, n. 2, p. 59-66, 2009.N/AHasVersion1678-4618N/AHasVersion0100-4670N/AHasVersion2-s2.0-85116836202N/AHasVersionhttps://doi.org/http://dx.doi.org/10.26850/1678-4618EQJ.V34.2.2009.P59-66DOIhttp://hdl.handle.net/11449/222610Handlehttps://doi.org/10.26850/1678-4618EQJ.V34.2.2009.P59-66DOI2022-04-28T19:45:47Z2022-04-282009-01-01T00:00:00ZGold electrodes are widely used in electrochemistry and electroanalytical chemistry, due to the high purity, broad range of work potential as well as the possibility to control and modify the surface. On this work construction and cleaning of electrodes from gold recordables compact discs (CD-Rs), namely CDtrodes, are described. The CDs was submitted to the action of concentrated HNO3 in order to remove the protection layer and to expose the metallic layer; the electrode area was delimited by using galvanoplasty tape. The literature has been published many articles on CDtrode focused on the application but not on the cleaning; there is no register on galvanoplasty tape to define electrode area. Several methods for gold surface cleaning after attack of HNO3 were investigated, such as application of fixed potential in NaCl solution, successive scans in H2SO4 and ultrasound application, and best results were obtained in H2SO4 solution. This electrode material is interesting due to the performance comparable to the commercial electrodes, besides great versatility and low cost.por59-66reponame:Repositório Institucional da UNESPinstname:Universidade Estadual Paulista (UNESP)instacron:UNESPjournal articlehttp://purl.org/coar/resource_type/c_6501literatureVoRhttp://purl.org/coar/version/c_970fb48d4fbd8a85 |
| spellingShingle | Avaliação da limpeza de CDtrodo construídos a partir de CD de ouro gravável/fita adesiva de galvanoplastia Foguel, M. V. CDtrode, CD-R electrodes Cyclic voltammetry Gold surface cleaning |
| status | SINGLETON |
| status_str | VoR |
| subject.fl_str_mv | CDtrode, CD-R electrodes Cyclic voltammetry Gold surface cleaning |
| title | Avaliação da limpeza de CDtrodo construídos a partir de CD de ouro gravável/fita adesiva de galvanoplastia |
| title_full | Avaliação da limpeza de CDtrodo construídos a partir de CD de ouro gravável/fita adesiva de galvanoplastia |
| title_fullStr | Avaliação da limpeza de CDtrodo construídos a partir de CD de ouro gravável/fita adesiva de galvanoplastia |
| title_full_unstemmed | Avaliação da limpeza de CDtrodo construídos a partir de CD de ouro gravável/fita adesiva de galvanoplastia |
| title_short | Avaliação da limpeza de CDtrodo construídos a partir de CD de ouro gravável/fita adesiva de galvanoplastia |
| title_sort | Avaliação da limpeza de CDtrodo construídos a partir de CD de ouro gravável/fita adesiva de galvanoplastia |
| topic | CDtrode, CD-R electrodes Cyclic voltammetry Gold surface cleaning |
| topic_facet | CDtrode, CD-R electrodes Cyclic voltammetry Gold surface cleaning |
| url | http://hdl.handle.net/11449/222610 |
| visible | 1 |
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