Publication
Effect of Glycerol Addition on Copper Electrodeposition on Steel Substrate
| Summary: | Abstract This work investigates the effect of the addition of glycerol on the microstructure, corrosion resistance, and efficiency of the electrodeposition process of Cu coating in an acid sulphate solution. The morphology and microstructures of electrodeposits were analyzed using Scanning Electron Microscopy (SEM), Spectrometry X-Ray Diffraction (XRD) and laser scanning confocal microscopy (LSCM). Evaluation of the corrosion resistance was performed in 2.0 mol⋅L−1 NaCl by means of weight loss tests and electrochemical techniques. The addition of glycerol resulted in a decrease in grain and crystallite sizes, a decrease in roughness and an increase in the tensile strain of the coating. The deposition efficiency and the corrosion resistance increased with the addition of glycerol exhibiting a maximum value at the concentration of 0.42 mol⋅L−1, increasing the efficiency of electrodeposition by approximately 96%. This is related to the roughness of the coating, which is minimal at this concentration. |
|---|---|
| Main Authors: | Barbosa,Rafael Santos |
| Other Authors: | Koga,Guilherme Yuuki; Nascimento,Marcio Luis Ferreira; Souza,Carlos Alberto Caldas de |
| Subject: | Cu coating glycerol electrodeposition corrosion |
| Year: | 2022 |
| Country: | Brazil |
| Document type: | article |
| Access type: | open access |
| Associated institution: | IBICT |
| Language: | English |
| Origin: | Oasisbr |
| _version_ | 1871510439134756864 |
|---|---|
| author | Barbosa,Rafael Santos |
| author2 | Koga,Guilherme Yuuki Nascimento,Marcio Luis Ferreira Souza,Carlos Alberto Caldas de |
| author2_role | author author author |
| author_facet | Barbosa,Rafael Santos Koga,Guilherme Yuuki Nascimento,Marcio Luis Ferreira Souza,Carlos Alberto Caldas de |
| author_role | author |
| country_str | BR |
| creators_json_txt | [{\"Person.name\":\"Barbosa,Rafael Santos\"},{\"Person.name\":\"Koga,Guilherme Yuuki\"},{\"Person.name\":\"Nascimento,Marcio Luis Ferreira\"},{\"Person.name\":\"Souza,Carlos Alberto Caldas de\"}] |
| datacite.creators.creator.creatorName.fl_str_mv | Barbosa,Rafael Santos Koga,Guilherme Yuuki Nascimento,Marcio Luis Ferreira Souza,Carlos Alberto Caldas de |
| datacite.rights.fl_str_mv | http://purl.org/coar/access_right/c_abf2 |
| datacite.subjects.subject.fl_str_mv | Cu coating glycerol electrodeposition corrosion |
| datacite.titles.title.fl_str_mv | Effect of Glycerol Addition on Copper Electrodeposition on Steel Substrate |
| dc.creator.none.fl_str_mv | Barbosa,Rafael Santos Koga,Guilherme Yuuki Nascimento,Marcio Luis Ferreira Souza,Carlos Alberto Caldas de |
| dc.format.none.fl_str_mv | text/html |
| dc.identifier.none.fl_str_mv | http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392022000100329 |
| dc.language.none.fl_str_mv | eng |
| dc.publisher.none.fl_str_mv | ABM, ABC, ABPol |
| dc.rights.none.fl_str_mv | http://purl.org/coar/access_right/c_abf2 |
| dc.source.none.fl_str_mv | Materials Research v.25 2022 reponame:Materials research (São Carlos. Online) instname:Universidade Federal de São Carlos (UFSCAR) instacron:ABM ABC ABPOL |
| dc.subject.none.fl_str_mv | Cu coating glycerol electrodeposition corrosion |
| dc.title.fl_str_mv | Effect of Glycerol Addition on Copper Electrodeposition on Steel Substrate |
| dc.type.none.fl_str_mv | http://purl.org/coar/resource_type/c_6501 |
| description | Abstract This work investigates the effect of the addition of glycerol on the microstructure, corrosion resistance, and efficiency of the electrodeposition process of Cu coating in an acid sulphate solution. The morphology and microstructures of electrodeposits were analyzed using Scanning Electron Microscopy (SEM), Spectrometry X-Ray Diffraction (XRD) and laser scanning confocal microscopy (LSCM). Evaluation of the corrosion resistance was performed in 2.0 mol⋅L−1 NaCl by means of weight loss tests and electrochemical techniques. The addition of glycerol resulted in a decrease in grain and crystallite sizes, a decrease in roughness and an increase in the tensile strain of the coating. The deposition efficiency and the corrosion resistance increased with the addition of glycerol exhibiting a maximum value at the concentration of 0.42 mol⋅L−1, increasing the efficiency of electrodeposition by approximately 96%. This is related to the roughness of the coating, which is minimal at this concentration. |
| dirty | 0 |
| eu_rights_str_mv | openAccess |
| format | article |
| id | oasisbr_a76e881163cb5bc8a32b77fefaa57b82 |
| identifier.url.fl_str_mv | http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392022000100329 |
| inst_facet_str | urn:organizationAcronym:oasisbr{{{_:::_}}}IBICT |
| instacron_str | OASISBR |
| institution | IBICT |
| instname_str | IBICT |
| language | eng |
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| oai_identifier_str | oai:scielo:S1516-14392022000100329 |
| organization_str_mv | urn:organizationAcronym:oasisbr |
| person_str_mv | Barbosa,Rafael Santos Koga,Guilherme Yuuki Nascimento,Marcio Luis Ferreira Souza,Carlos Alberto Caldas de |
| publishDate | 2022 |
| publisher.none.fl_str_mv | ABM, ABC, ABPol |
| repo_facet_str | urn:repositoryAcronym:oasisbr{{{_:::_}}}Oasisbr |
| reponame_str | Oasisbr |
| repository_id_str | urn:repositoryAcronym:oasisbr |
| service_str_mv | urn:repositoryAcronym:oasisbr |
| spelling | Effect of Glycerol Addition on Copper Electrodeposition on Steel SubstrateBarbosa,Rafael SantosKoga,Guilherme YuukiNascimento,Marcio Luis FerreiraSouza,Carlos Alberto Caldas deCu coatingglycerolelectrodepositioncorrosionopen accesshttp://purl.org/coar/access_right/c_abf2http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392022000100329URLhttp://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392022000100329URLHasVersion2022-01-01Abstract This work investigates the effect of the addition of glycerol on the microstructure, corrosion resistance, and efficiency of the electrodeposition process of Cu coating in an acid sulphate solution. The morphology and microstructures of electrodeposits were analyzed using Scanning Electron Microscopy (SEM), Spectrometry X-Ray Diffraction (XRD) and laser scanning confocal microscopy (LSCM). Evaluation of the corrosion resistance was performed in 2.0 mol⋅L−1 NaCl by means of weight loss tests and electrochemical techniques. The addition of glycerol resulted in a decrease in grain and crystallite sizes, a decrease in roughness and an increase in the tensile strain of the coating. The deposition efficiency and the corrosion resistance increased with the addition of glycerol exhibiting a maximum value at the concentration of 0.42 mol⋅L−1, increasing the efficiency of electrodeposition by approximately 96%. This is related to the roughness of the coating, which is minimal at this concentration.engtext/htmlABM, ABC, ABPolMaterials Research v.25 2022reponame:Materials research (São Carlos. Online)instname:Universidade Federal de São Carlos (UFSCAR)instacron:ABM ABC ABPOLjournal articlehttp://purl.org/coar/resource_type/c_6501literatureVoRhttp://purl.org/coar/version/c_970fb48d4fbd8a85 |
| spellingShingle | Effect of Glycerol Addition on Copper Electrodeposition on Steel Substrate Barbosa,Rafael Santos Cu coating glycerol electrodeposition corrosion |
| status | SINGLETON |
| status_str | VoR |
| subject.fl_str_mv | Cu coating glycerol electrodeposition corrosion |
| title | Effect of Glycerol Addition on Copper Electrodeposition on Steel Substrate |
| title_full | Effect of Glycerol Addition on Copper Electrodeposition on Steel Substrate |
| title_fullStr | Effect of Glycerol Addition on Copper Electrodeposition on Steel Substrate |
| title_full_unstemmed | Effect of Glycerol Addition on Copper Electrodeposition on Steel Substrate |
| title_short | Effect of Glycerol Addition on Copper Electrodeposition on Steel Substrate |
| title_sort | Effect of Glycerol Addition on Copper Electrodeposition on Steel Substrate |
| topic | Cu coating glycerol electrodeposition corrosion |
| topic_facet | Cu coating glycerol electrodeposition corrosion |
| url | http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392022000100329 |
| visible | 1 |
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