Publication
Electrodeposition of Ni-Mo and Fe-Mo alloys from sulfate-citrate acid solutions
| Summary: | This paper reports on a study of the electrodeposition of Ni-Mo and Fe-Mo alloys on Pt electrodes in a sodium citrate solution at pH 4.0. The alloys were subjected to cyclic voltammetry at different ion concentration ratios to identify their behavior. The electrodeposited coatings were analyzed by SEM, EDX and XRD. The results of the cyclic voltammetry tests indicated the presence of dissolution peaks only with high Ni or Fe ion concentrations. The SEM analysis revealed that the two alloys had dissimilar morphologies and the Ni-Mo alloys were homogeneous and thick. The Mo and O contents were higher in the Ni-Mo than in the Fe-Mo alloys. Anomalous deposition was found to occur in the co-deposition of Ni and Mo. |
|---|---|
| Main Authors: | Sanches,Luciana S. |
| Other Authors: | Domingues,Sergio H.; Carubelli,Ademir; Mascaro,Lucia H. |
| Subject: | electrodeposition Ni-Mo alloys Fe-Mo alloys |
| Year: | 2003 |
| Country: | Brazil |
| Document type: | article |
| Access type: | open access |
| Associated institution: | IBICT |
| Language: | English |
| Origin: | Oasisbr |
| _version_ | 1871506519360536576 |
|---|---|
| author | Sanches,Luciana S. |
| author2 | Domingues,Sergio H. Carubelli,Ademir Mascaro,Lucia H. |
| author2_role | author author author |
| author_facet | Sanches,Luciana S. Domingues,Sergio H. Carubelli,Ademir Mascaro,Lucia H. |
| author_role | author |
| country_str | BR |
| creators_json_txt | [{\"Person.name\":\"Sanches,Luciana S.\"},{\"Person.name\":\"Domingues,Sergio H.\"},{\"Person.name\":\"Carubelli,Ademir\"},{\"Person.name\":\"Mascaro,Lucia H.\"}] |
| datacite.creators.creator.creatorName.fl_str_mv | Sanches,Luciana S. Domingues,Sergio H. Carubelli,Ademir Mascaro,Lucia H. |
| datacite.rights.fl_str_mv | http://purl.org/coar/access_right/c_abf2 |
| datacite.subjects.subject.fl_str_mv | electrodeposition Ni-Mo alloys Fe-Mo alloys |
| datacite.titles.title.fl_str_mv | Electrodeposition of Ni-Mo and Fe-Mo alloys from sulfate-citrate acid solutions |
| dc.creator.none.fl_str_mv | Sanches,Luciana S. Domingues,Sergio H. Carubelli,Ademir Mascaro,Lucia H. |
| dc.format.none.fl_str_mv | text/html |
| dc.identifier.none.fl_str_mv | http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532003000400011 |
| dc.language.none.fl_str_mv | eng |
| dc.publisher.none.fl_str_mv | Sociedade Brasileira de Química |
| dc.rights.none.fl_str_mv | http://purl.org/coar/access_right/c_abf2 |
| dc.source.none.fl_str_mv | Journal of the Brazilian Chemical Society v.14 n.4 2003 reponame:Journal of the Brazilian Chemical Society (Online) instname:Sociedade Brasileira de Química (SBQ) instacron:SBQ |
| dc.subject.none.fl_str_mv | electrodeposition Ni-Mo alloys Fe-Mo alloys |
| dc.title.fl_str_mv | Electrodeposition of Ni-Mo and Fe-Mo alloys from sulfate-citrate acid solutions |
| dc.type.none.fl_str_mv | http://purl.org/coar/resource_type/c_6501 |
| description | This paper reports on a study of the electrodeposition of Ni-Mo and Fe-Mo alloys on Pt electrodes in a sodium citrate solution at pH 4.0. The alloys were subjected to cyclic voltammetry at different ion concentration ratios to identify their behavior. The electrodeposited coatings were analyzed by SEM, EDX and XRD. The results of the cyclic voltammetry tests indicated the presence of dissolution peaks only with high Ni or Fe ion concentrations. The SEM analysis revealed that the two alloys had dissimilar morphologies and the Ni-Mo alloys were homogeneous and thick. The Mo and O contents were higher in the Ni-Mo than in the Fe-Mo alloys. Anomalous deposition was found to occur in the co-deposition of Ni and Mo. |
| dirty | 0 |
| eu_rights_str_mv | openAccess |
| format | article |
| id | oasisbr_35e655e32bb611f5ad280a4f0044f053 |
| identifier.url.fl_str_mv | http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532003000400011 |
| inst_facet_str | urn:organizationAcronym:oasisbr{{{_:::_}}}IBICT |
| instacron_str | OASISBR |
| institution | IBICT |
| instname_str | IBICT |
| language | eng |
| network_acronym_str | oasisbr |
| network_name_str | Oasisbr |
| oai_identifier_str | oai:scielo:S0103-50532003000400011 |
| organization_str_mv | urn:organizationAcronym:oasisbr |
| person_str_mv | Sanches,Luciana S. Domingues,Sergio H. Carubelli,Ademir Mascaro,Lucia H. |
| publishDate | 2003 |
| publisher.none.fl_str_mv | Sociedade Brasileira de Química |
| repo_facet_str | urn:repositoryAcronym:oasisbr{{{_:::_}}}Oasisbr |
| reponame_str | Oasisbr |
| repository_id_str | urn:repositoryAcronym:oasisbr |
| service_str_mv | urn:repositoryAcronym:oasisbr |
| spelling | Electrodeposition of Ni-Mo and Fe-Mo alloys from sulfate-citrate acid solutionsSanches,Luciana S.Domingues,Sergio H.Carubelli,AdemirMascaro,Lucia H.electrodepositionNi-Mo alloysFe-Mo alloysopen accesshttp://purl.org/coar/access_right/c_abf2http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532003000400011URLhttp://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532003000400011URLHasVersion2003-08-01This paper reports on a study of the electrodeposition of Ni-Mo and Fe-Mo alloys on Pt electrodes in a sodium citrate solution at pH 4.0. The alloys were subjected to cyclic voltammetry at different ion concentration ratios to identify their behavior. The electrodeposited coatings were analyzed by SEM, EDX and XRD. The results of the cyclic voltammetry tests indicated the presence of dissolution peaks only with high Ni or Fe ion concentrations. The SEM analysis revealed that the two alloys had dissimilar morphologies and the Ni-Mo alloys were homogeneous and thick. The Mo and O contents were higher in the Ni-Mo than in the Fe-Mo alloys. Anomalous deposition was found to occur in the co-deposition of Ni and Mo.engtext/htmlSociedade Brasileira de QuímicaJournal of the Brazilian Chemical Society v.14 n.4 2003reponame:Journal of the Brazilian Chemical Society (Online)instname:Sociedade Brasileira de Química (SBQ)instacron:SBQjournal articlehttp://purl.org/coar/resource_type/c_6501literatureVoRhttp://purl.org/coar/version/c_970fb48d4fbd8a85 |
| spellingShingle | Electrodeposition of Ni-Mo and Fe-Mo alloys from sulfate-citrate acid solutions Sanches,Luciana S. electrodeposition Ni-Mo alloys Fe-Mo alloys |
| status | SINGLETON |
| status_str | VoR |
| subject.fl_str_mv | electrodeposition Ni-Mo alloys Fe-Mo alloys |
| title | Electrodeposition of Ni-Mo and Fe-Mo alloys from sulfate-citrate acid solutions |
| title_full | Electrodeposition of Ni-Mo and Fe-Mo alloys from sulfate-citrate acid solutions |
| title_fullStr | Electrodeposition of Ni-Mo and Fe-Mo alloys from sulfate-citrate acid solutions |
| title_full_unstemmed | Electrodeposition of Ni-Mo and Fe-Mo alloys from sulfate-citrate acid solutions |
| title_short | Electrodeposition of Ni-Mo and Fe-Mo alloys from sulfate-citrate acid solutions |
| title_sort | Electrodeposition of Ni-Mo and Fe-Mo alloys from sulfate-citrate acid solutions |
| topic | electrodeposition Ni-Mo alloys Fe-Mo alloys |
| topic_facet | electrodeposition Ni-Mo alloys Fe-Mo alloys |
| url | http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532003000400011 |
| visible | 1 |
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