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  1. 1

    In vitro wear resistance of three types of polymethyl methacrylate denture teeth

    Publicação
    por Reis, Katia Rodrigues
    Outros Autores: Bonfante, Gerson; Pegoraro, Luiz Fernando; Conti, Paulo Cesar Rodrigues; Oliveira, Pedro Cesar Garcia de; Kaizer, Osvaldo Bazzan
    Origem: Oasisbr
    The wear resistance of denture teeth is important to the longevity of removable prostheses of edentulous patients. The ability of denture teeth to maintain a stable occlusal relationship over time may be influenced by this property. The purpose of this in vitro study was to evaluate the wear resistance of polymethyl methacrylate (PMMA) denture teeth based on their chemical composition when opposed by a ceramic antagonist. The maxillary canines (n=10) of 3 PMMA denture teeth (Trubyte Biotone, cross-linked PMMA; Trilux, highly cross-linked IPN (interpenetrating polymer network)-PMMA; and Vivodent, highly cross-linked PMMA) were secured in an in vitro 2-body wear-testing apparatus that produced sliding contact of the specimens (4.5 cycles/s, sliding distance of 20 mm, under 37°C running water) against glazed or airborne particle abraded ceramic. Wear resistance was measured as height loss (mm) under 300 g (sliding force) after 100,000 cycles, using a digital measuring microscope. Mean values were analyzed by 2-way ANOVA and Tukey's test (a=0.05). The wear of Trubyte Biotone (0.93 ± 0.14 mm) was significantly higher than that of both other types of teeth tested against abraded ceramic (p;0.05) in wear among the 3 denture teeth evaluated against glazed ceramic. Trilux and Vivodent teeth tested against either glazed or airborne particle abraded ceramic did not differ significantly from each other (p
    2008 artigo Brasil
  2. 2

    Effect of repeated immersion solution cycles on the color stability of denture tooth acrylic resins

    Publicação
    por Silva, Paulo Maurício Batista da
    Outros Autores: Acosta, Emílio José Tabaré Rodríguez; Jacobina, Matheus; Pinto, Luciana de Rezende; Porto, Vinícius Carvalho
    Origem: Oasisbr
    OBJECTIVE: Chemical solutions have been widely used for disinfection of dentures, but their effect on color stability of denture tooth acrylic resins after repeated procedures is still unclear. The aim of this in vitro study was to evaluate whether repeated cycles of chemical disinfectants affected the color stability of two denture tooth acrylic resins. MATERIAL AND METHODS: Sixty disc-shaped specimens (40 mm x 3 mm) were fabricated from two different brands (Artiplus and Trilux) of denture tooth acrylic resin. The specimens from each brand (n=30) were randomly divided into 6 groups (n=5) and immersed in the following solutions: distilled water (control group) and 5 disinfecting solutions (1% sodium hypochlorite, 2% sodium hypochlorite, 5.25% sodium hypochlorite, 2% glutaraldehyde, and 4% chlorhexidine gluconate). Tooth color measurements were made by spectrophotometry. Before disinfection, the initial color of each tooth was recorded. Further color measurements were determined after subjecting the specimens to 7, 21, 30, 45, 60, and 90 immersion cycles in each tested solution. Color differences (ΔE*) were determined using the CIE L*a*b* color system. Data were analyzed using two-way repeated measures analysis of variance (ANOVA) followed by Tukey tests. The significance level was set at 5%. RESULTS: There were statistically significant differences in ΔE* among the 5 disinfectants and water during the 90 cycles of immersion for both denture tooth acrylic resins. Distilled water promoted the greatest color change in both denture tooth acrylic resins, nevertheless none of tested disinfectants promoted ΔE* values higher than 1.0 on these acrylic materials during the 90 cycles of disinfection. CONCLUSIONS: Repeated immersion cycles in disinfecting solutions alter ΔE* values, however these values do not compromise the color of the tested denture tooth acrylic resins because they are imperceptible to the human eye.
    2011 artigo Brasil
  3. 3

    Bond strength between acrylic resin and maxillofacial silicone

    Publicação
    por Haddad, Marcela Filié
    Outros Autores: Goiato, Marcelo Coelho; Santos, Daniela Micheline dos; Crepaldi, Nádia de Marchi; Pesqueira, Aldiéris Alves; Bannwart, Lisiane Cristina
    Origem: Oasisbr
    The development of implant dentistry improved the possibilities of rehabilitation with maxillofacial prosthesis. However, clinically it is difficult to bond the silicone to the attachment system. OBJECTIVES: This study aimed to evaluate the effect of an adhesive system on the bond strength between acrylic resin and facial silicone. MATERIAL AND METHODS: A total of 120 samples were fabricated with auto-polymerized acrylic resin and MDX 4-4210 facial silicone. Both materials were bonded through mechanical retentions and/or application of primers (DC 1205 primer and Sofreliner primer S) and adhesive (Silastic Medical Adhesive Type A) or not (control group). Samples were divided into 12 groups according to the method used to attach the silicone to the acrylic resin. All samples were subjected to a T-peel test in a universal testing machine. Failures were classified as adhesive, cohesive or mixed. The data were evaluated by the analysis of variance (ANOVA) and the Tukey's HSD test (α=.05). RESULTS: The highest bond strength values (5.95 N/mm; 3.07 N/mm; 4.75 N/mm) were recorded for the samples that received a Sofreliner primer application. These values were significantly higher when the samples had no scratches and did not receive the application of Silastic Medical Adhesive Type A. CONCLUSIONS: The most common type of failure was adhesive. The use of Sofreliner primer increased the bond strength between the auto-polymerized acrylic resin and the Silastic MDX 4-4210 facial silicone.
    2012 artigo Brasil
  4. 4

    The effect of microplastics pollution in microalgal biomass production: a biochemical study

    Publicação
    por Cunha, César
    Outros Autores: Lopes, Joana; Paulo, Jorge; Faria, Marisa; Kaufmann, Manfred; Nogueira, Natacha et al.
    Microplastics (MPs) are widely spread throughout aquatic systems and water bodies. Given that water quality is one of the most important parameters in the microalgal-based industry, it is critical to assess the biochemical impact of short- and long-term exposure to MPs pollution. Here, the microalga Phaeodactylum tricornutum was exposed to water contaminated with 0.5 and 50 mg L-1 of polystyrene (PS) and/or polymethyl methacrylate (PMMA). Results show that the microalgal cultures exposed to lower concentrations of PS displayed a growth enhancement of up to 73% in the first stage (days 3-9) of the exponential growth phase. Surprisingly, and despite the fact that long-term exposure to MPs contamination did not impair microalgal growth, a steep decrease in biomass production (of up to 82%) was observed. The production of photosynthetic pigments was shown to be pH-correlated during the full growth cycle, but cell density-independent in later stages of culturing. The extracellular carbohydrates production exhibited a major decrease during long-term exposure. Still, the production of extracellular proteins was not affected by the presence of MPs. This pilot laboratory-scale study shows that the microalgal exposure to water contaminated with MPs disturbs its biochemical equilibrium in a time-dependent manner, decreasing biomass production. Thus, microalgal industry-related consequences derived from the use of MPs-contaminated water are a plausible possibility.
    2020 artigo Portugal acesso aberto
  5. 5

    Antimicrobial activity of a 3D-printed polymethylmethacrylate dental resin enhanced with graphene

    Publicação
    por Salgado, Helena
    Outros Autores: Gomes, Ana T. P. C.; Duarte, Ana S.; Ferreira, José M. F.; Fernandes, Carlos; Figueiral, Maria Helena et al.
    The present study aimed to test, in vitro, the antimicrobial activity against Candida albicans and Streptococcus mutans and the surface roughness of a 3D-printed polymethylmethacrylate dental resin enhanced with graphene. A 3D-printed polymethylmethacrylate dental resin was reinforced with four different concentrations of graphene: 0.01, 0.1, 0.25 and 0.5 wt%. Neat resin was used as a control. The specimens were printed in a liquid crystal display printer. Disc specimens were used in antimicrobial evaluation, and bar-shaped specimens were used to measure surface roughness. The study of antimicrobial activity included the inhibition of the growth of C. albicans and S. mutans and their adhesion to the resin’s surface. Surface roughness increased with the increase in the graphene concentration. The growth inhibition of C. albicans was observed in the different concentrations of graphene after 24 h, with no recovery after 48 h. The specimens doped with graphene were capable of inactivating S. mutans after 48 h. The surface-adhesion studies showed that the density of microbial biofilms decreases in the case of specimens doped with graphene. Graphene, despite increasing the resin’s surface roughness, was effective in inhibiting the growth and the adhesion to the resin’s surface of the main inducers of prosthetic stomatitis.
    2022 artigo Portugal acesso aberto
  6. 6

    The antimicrobial effect of the incorporation of inorganic substances into heat-cured denture base resins - a systematic review

    Publicação
    por Lima, Mariana
    Outros Autores: Salgado, Helena; Correia, André; Fonseca, Patrícia
    Introduction: Polymethylmethacrylate (PMMA) is the most widely used denture base material due to its favourable properties. Several studies have tested the incorporation of anti-infective agents into PMMA as a strategy to prevent biofilm growth on the denture surface. This systematic review aims to evaluate the efficacy of incorporating inorganic antimicrobial particles into denture base resins in preventing antimicrobial growth, thereby identifying the most effective agents for enhancing PMMA’s antimicrobial properties. Materials and methods: This systematic review followed the PRISMA guidelines, and the research protocol was registered in PROSPERO. The search was performed by using Medical Subject Headings and free text combined with Boolean operators in PubMed/Medline® and in Cochrane® and a free text combination in Web of Science® Core Collection. Data regarding the inorganic particles studied, their antimicrobial effect, and the type of samples produced were collected and analysed. Results: After screening, a total of fifteen studies were included in this review. Most samples were disk-shaped and of varying sizes, and the most tested microbial strain was Candida albicans. Silver was the most used antimicrobial particle, followed by gold, titanium, and copper. Conclusions: Overall, incorporating inorganic particles into PMMA has produced promising antimicrobial results, depending on the concentration. Due to the high heterogeneity observed in the samples, more studies are recommended, particularly clinical trials.
    2024 artigo de revisão Portugal acesso aberto
  7. 7

    Mechanical properties of polymethyl methacrylate as denture base material: heat-polymerized vs. 3D-printed — systematic review and meta-analysis of in vitro studies

    Publicação
    por Lourinho, Cláudia
    Outros Autores: Salgado, Helena; Correia, André; Fonseca, Patrícia
    The synergy between dentistry and informatics has allowed the emergence of new technologies, specifically 3D printing, which has led to the development of new materials. The aim of this research was to compare the mechanical properties of dental base resins for 3D printing with conventional ones. This systematic review was developed using the PRISMA guidelines, and the electronic literature search was performed with the PubMed/MEDLINE, Web of Science—MEDLINE and EMBASE databases, until 30 April 2022. Two researchers selected the studies independently, and thus eight articles were found eligible for analysis. A meta-analysis was developed to estimate flexural strength. The Cohen’s kappa corresponding to this review was 1.00, and the risk assessment was considered low for the included studies. The 3D printing resin presented lower values of flexural strength and hardness compared with the heat-cured resin. Regarding impact strength, a lower value was recorded for the heat-cured resin compared with the 3D printing resin. Three-dimensional printing resins are viable materials for making prosthetic bases but need further clinical research.
    2022 artigo Portugal acesso aberto
  8. 8

    A different approach to analyzing the surface roughness of prosthetic dental acrylic resins

    Publicação
    por Quezada, Margarida Martins
    Outros Autores: Fernandes, Carlos; Montero, Javier; Correia, André; Salgado, Helena; Fonseca, Patrícia
    (1) Introduction: Apart from the polishing method, conventional or mechanized, the arithmetic mean roughness (Ra) is the most common metric to evaluate the surface roughness of denture base acrylic resins. An overview of the constraints related to this roughness parameter is highlighted in this study. This research introduces new parameters for accessing a functional analysis of surface roughness. (2) Materials and Methods: Five samples of CAD/CAM 3D-printed acrylic resins were prepared. Two polishing techniques, manual and mechanical, were applied. Surface roughness parameters were extracted from a profilometer reading: arithmetic mean height (Ra and Pa), skewness (Rsk and Psk), and kurtosis (Rku and Pku). (3) Results: Significant differences (p < 0.001) were found in the Ra distribution among the study samples, in contrast with the lack of significance in Pa values. Surface roughness parameters revealed an increased coefficient of variance (CV) value due to mechanized polishing across the specimens analyzed. Skewness and kurtosis indicate a more pronounced distribution with the manual polishing technique. (4) Conclusion: This preliminary study exhibits the influence of different polishing protocols on surface roughness parameters. The primary profile, skewness, and kurtosis should be assessed for the surface characterization of acrylic resins.
    2024 artigo Portugal acesso aberto
  9. 9

    Investigation of the effect of the same polishing protocol on the surface roughness of denture base acrylic resins

    Publicação
    por Quezada, Margarida Martins
    Outros Autores: Salgado, Helena; Correia, André; Fernandes, Carlos; Fonseca, Patrícia
    This investigation aims to determine the effect of the same polishing protocol on the surface roughness (Ra) of different resins obtained by different processing techniques. Acrylic resins obtained by CAD/CAM technology overcame the disadvantages identified in conventional materials. A total of thirty samples (six of each resin): self-cured, heat-polymerized, injection molded, CAD/CAM 3D-printed and CAD/CAM milled were prepared. JOTA ®  Kit 1877 DENTUR POLISH was used to polish the samples by two techniques: manual and mechanized, with a prototype for guided polishing exclusively developed for this investigation. The Ra was measured by a profilometer. The values were analyzed using ANOVA, Games-Howell post-hoc test and One-sample t-test, with p < 0.05. Manual polishing produces lower values of Ra compared to mechanized polishing, except for injected molded resins ( p = 0.713). Manual polishing reveals significant differences between the resin pairs milling/3D-printing ( p = 0.012) and thermopolymerizable/milling ( p = 0.024). In the mechanized technique only, significant differences regarding the R a values were found between the self-cured/3D-printed ( p = 0.004) and self-cured/thermopolymerizable pair resins ( p = 0.004). Differences in surface roughness values can be attributed to the inherent characteristics of the resin and the respective processing techniques.
    2022 artigo Portugal acesso aberto
  10. 10

    Influence of popular beverages on the fracture resistance of implant-supported bis-acrylic resin provisional crowns: an in vitro study

    Publicação
    por Ribera, Oriana Karolina Caldeira
    Implant-supported provisional restorations are critical for improving the esthetics and shaping of the peri-implant tissue. The mechanical properties of these provisional materials can be influenced by saliva, food, beverages, and interactions between these materials in the oral environment. Therefore, integrity of provisional restorations should be preserved throughout the treatment period. This study aimed to evaluate the fracture strength of implant-supported polymethyl methacrylate (PMMA) provisional restorations made of computer-aided design and computer-aided manufacturing when immersed in different solutions at a controlled temperature of 37° C for 7 days. Each analog-pillar-crown set was submerged in different liquids (distilled water, tea, coffee, red wine, and Coca Cola®) for 1 week at a controlled oral temperature of 37° C. The samples were then subjected to fracture forces. The moment of fracture of the crown was recorded and compared with those of the other samples. Specimens immersed in distilled water (control group) had the highest fracture resistance (mean [M]=1331.00, standard deviation [SD]=296.74), while those immersed in tea had the lowest mean strength to fracture (M=967.00, SD=281.86). Nutritional deficiency and inappropriate eating habits influence the fracture strength of temporary crowns, rendering them more elastic or less resistant to fractures.
    2023 dissertação de mestrado Portugal acesso aberto